Analytical Chemistry volume 1

Cover Analytical Chemistry volume 1
Analytical Chemistry volume 1
F P Frederick Pearson Treadwell
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P. 399).
Detection of Nitric Acid in the Presence of Nitrous Acid With the exception of the Lunge-Lwoff method, there is no absolutely reliable qualitative test for the detection of traces of nitric acid in the presence of large amounts of nitrous acid in aqueous solution. A number of methods have been proposed which depend upon the destruction of the nitrous acid by diazotizing, but they all yield only approximate results; because, in order to destroy the nitrous acid, it is necessary first to
... set the acid itself free by the addition of another acid, which always causes a part of the nitrous acid to be changed to nitric acid ; so that the latter will be detected even when no nitric acid was originally present.
Large amounts of nitric acid in the presence of nitrous acid may be detected by the method proposed by Piccini, t in which a concentrated solution containing * LUNGE, Z. Angew. Chemie, 1894, 348. F Z. Anal. Chem. , 19, 354.
396 'REACTIONS OF THE ACID CONSTITUENTS salts of both acids is treated with a concentrated solution of urea, and then covered (by means of a pipette) with dilute sulfuric acid.


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