Aromatic Carbene Transition Metal Complexes
Aromatic Carbene Transition Metal Complexes
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After an additional 0.5 hour of reflux, the mixture was allowed to stand at room temperature over- night.
The mixture was twice extracted with 200 ml portions of petroleum ether. The organic extracts were dried over anhydrous magnesium sulfate and the solvent was removed in vacuo (rotary evaporator) . The residue was vacuum dis- tilled. This distillate was a mixture of dihydronaphthalene, tetralin, and naphthalene. The amount of the dihydronaph- thalene (0.610 moles) was determined by nmr integ...ration.
Preparation of l,2-benzo-4- and 1, 2-benzo-6-broraocyclo - heptatrienes (4S, 49) . A mixture of naphthalene, tetra- hydrcnaphthalene , dihydronaphthalene (0.610 moles in a 218 g mixture), benzyltriethylammonium chloride (0.8 g) , and bromo- form 459.4 g (1.8 moles) was mechanically stirred and cooled with a water bath. To this mixture, 500 g of 50% w/w aqueous sodium hydroxide was added dropwise. After 24 hours of stirring, 50 ml of H o was added and the organic layer was washed twice with 250 ml portions of water.
What to read after Aromatic Carbene Transition Metal Complexes?
You can find similar books in the "Read Also" column, or choose other free books by Allison, Neil Thomas to read onlineMoreLess
To quickly assess the difficulty of the text, read a short excerpt:
After an additional 0.5 hour of reflux, the mixture was allowed to stand at room temperature over- night.
The mixture was twice extracted with 200 ml portions of petroleum ether. The organic extracts were dried over anhydrous magnesium sulfate and the solvent was removed in vacuo (rotary evaporator) . The residue was vacuum dis- tilled. This distillate was a mixture of dihydronaphthalene, tetralin, and naphthalene. The amount of the dihydronaph- thalene (0.610 moles) was determined by nmr integ...ration.
Preparation of l,2-benzo-4- and 1, 2-benzo-6-broraocyclo - heptatrienes (4S, 49) . A mixture of naphthalene, tetra- hydrcnaphthalene , dihydronaphthalene (0.610 moles in a 218 g mixture), benzyltriethylammonium chloride (0.8 g) , and bromo- form 459.4 g (1.8 moles) was mechanically stirred and cooled with a water bath. To this mixture, 500 g of 50% w/w aqueous sodium hydroxide was added dropwise. After 24 hours of stirring, 50 ml of H o was added and the organic layer was washed twice with 250 ml portions of water.
What to read after Aromatic Carbene Transition Metal Complexes?
You can find similar books in the "Read Also" column, or choose other free books by Allison, Neil Thomas to read onlineMoreLess
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