Determination of Lithium

Cover Determination of Lithium
Determination of Lithium
W W William Woolford Skinner
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In liis tests of the phosphate method he found Hthium even in the first filtrate upon taking up the soluble material from the precipitate.
Ranzoli ^ in a comparison of different methods of separation of lithium obtained the following errors: By Mayer's ^ phosphate method when working with quantities of from 0. 2452 to 0. 5200 gram, the losses were from 0. 0097 gram to 0. 0176 gram, equivalent to an average of 3. 05 per cent. By Carnot's ^ method he obtained 0. 4780 gram and 0. 4797 gram instead
... of 0. 5200, showing losses of 0. 0470 and 0. 0403 gram, or equivalent to 7. 9 per cent. By Gooch's * method he obtained 0. 4907 and 0. 4969 gram instead of 0. 5200, losses of 0. 0293 and 0. 0231 gram, or equivalent to 5 per cent. He said that all the gravimetric determinations were carried out wdth all the precautions recommended by the authors. Of course in the analysis of mineral waters one rarely has to deal wdth quantities of lithium sulphate as great as 0. 5 gram, and the quantity of mixed chlorids from a natural water which would contain such an amount of litliium would be entirely too large to handle as a matter of quantitative analysis.

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