Laboratory Work in Physiological Chemistry

Cover Laboratory Work in Physiological Chemistry
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The narrow tube thus obtained is cut up into pieces about five inches long; each of these fused in the middle yields two tubes which are used in making the determination. Fill one of these tubes, sealed at one end, to a height of % — yi inch with the substance, then fasten this by means of a small rubber band cut from a piece of rubber tubing, to a thermometer so that the sealed end of the tube is on a level with the end of the bulb of the thermometer.
Suspend the thermometer with the attached
...tube in a beaker of about 100 c.c. capacity, containing enough sulphuric acid to clear the substance in the tube as well as the bulb of the thermometer. Now heat with a small flame, stirring constantly, till the substance begins to melt. This is the melting-point; note the temperature.
Taste a specimen of pure urea? What is it like?
Examine the crystals of urea under the microscope; recrystallize, if necessary. Sketch the form of the crystals observed.
Test the solubility of the urea in water, alcohol and ether.


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Laboratory Work in Physiological Chemistry
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