Methods in Metallurgical Analysis
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When the steel is dis- solved add 5 cc. Of strong nitric acid. Evaporate until the sulphu- ric acid fumes, to destroy carbonaceous matter. Add 100 cc. Of water and boil to dissolve ferric sulphate. Transfer the solution to a 500-cc. Graduated flask. Add sodium carbonate solution until the solution of steel is dark in color and the pre- cipitate dissolves slowly. Add emulsion of zinc oxide, a little at a time, and shake until the iron and chromium are precipitated. Dilute to the mark with water.... Let the precipitate settle. Decant 250 cc. Through a dry filter into a quarter-liter graduated flask. Transfer it to a half-liter Erlenmeyer flask and acidify with 25 cc. Of nitric acid (sp. Gr. 1. 42). Add 1 gm. Of sodium bismuthate and shake the flask several minutes. Let the residue settle. Filter through asbestos with suction. Wash the flask and filter with water acidulated with nitric acid until the washings are free from the pink color of permanganic acid. Transfer the filtrate to a beaker, add a measured volume of standard ferrous sulphate solution in excess of the permanganic acid, and titrate the excess of ferrous sulphate with standard potassium per- * Met.
What to read after Methods in Metallurgical Analysis?
You can find similar books in the "Read Also" column, or choose other free books by Charles Henry White to read onlineMoreLess
To quickly assess the difficulty of the text, read a short excerpt:
When the steel is dis- solved add 5 cc. Of strong nitric acid. Evaporate until the sulphu- ric acid fumes, to destroy carbonaceous matter. Add 100 cc. Of water and boil to dissolve ferric sulphate. Transfer the solution to a 500-cc. Graduated flask. Add sodium carbonate solution until the solution of steel is dark in color and the pre- cipitate dissolves slowly. Add emulsion of zinc oxide, a little at a time, and shake until the iron and chromium are precipitated. Dilute to the mark with water.... Let the precipitate settle. Decant 250 cc. Through a dry filter into a quarter-liter graduated flask. Transfer it to a half-liter Erlenmeyer flask and acidify with 25 cc. Of nitric acid (sp. Gr. 1. 42). Add 1 gm. Of sodium bismuthate and shake the flask several minutes. Let the residue settle. Filter through asbestos with suction. Wash the flask and filter with water acidulated with nitric acid until the washings are free from the pink color of permanganic acid. Transfer the filtrate to a beaker, add a measured volume of standard ferrous sulphate solution in excess of the permanganic acid, and titrate the excess of ferrous sulphate with standard potassium per- * Met.
What to read after Methods in Metallurgical Analysis?
You can find similar books in the "Read Also" column, or choose other free books by Charles Henry White to read onlineMoreLess
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