Practical And Analytical Chemistry Being a Complete Course in Chemical Analysis

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fl by name test.
Ppt. Ca. White.
Filt. Mg, Mn. Evaporate a portion to dryness and test with borax bead for Mn.
To another por- tion add H 3 C 6 H 6 O 7, then NH 4 OH in excess and To the remaining portion add Fe 2 Cl e, filter out the Fe 2 (PO 4 ) 2, to filtrate add (NH 4 ) 2 C 2 4) NH 4 C1, NH 4 OH and NH 4 HS, white precipitate = Ce.
to separate Fa and Mn, filter and test filtrate with Na 2 HPO 4, white ppt. = Mg.
DIVISION I. When the bases are the alkali metals, and the re- action is neutral
....
RULE I. Evaporate a portion of the solution to dryness, and slowly heat to redness.
If the mass chars, one or more of the following organic acids are indicated : ACETATES, TARTRATES, CITRATES, GAL- LATES, TANNATES.
NOTE. Oxalates do not char, although if the heating take place slowly a grayish coloration may be noticed, the residue in this case giving off CO 2 on the addition of H 2 SO 4 .
Fe 2 Cl 6 immediately detects TANNATES and GALLATES. Gallic acid crystallizes in the cold on acidifying the solution.


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