The Brewers Analyst a Systematic Handbook of Analysis Relating to Brewing And

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C. Of this 10 per cent, solution ( = 2 c. C. Bisulphite) into a beaker, add about 150 c. C. Distilled water and about 10 c. C. Animonic oxalate, about the same quantity of ammonic chloride, and about the same quantity of ammonic hydrate. Gently warm the liquid and allow to remain at rest for about 3 hours and then filter. (The filtrate is required for the following magnesia estimation. ) Wash the precipitate with hot distilled water, dry, ignite, cool, recarbonate, heat gently, cool under desic...cator, and weigh as calcic carbonate (CaC0 3 ).
Example : Weight of crucible + ash . . . 6'588 grams. Weight of crucible .... 6 '500 0-088 0-088 x -56 = 0-049 CaO in 2 c. C. Bisulphite and x 50-2-450 lime (CaO) per 100 c. C.
5. Magnesia. To the filtrate from the previously described lime estimation add about 10 c. C. Ammonic or sodic phosphate and about a like amount of ammonic hydrate ; stir well and set aside for 6 hours. Now filter, wash the precipitate with dilute ammonia, dry, ignite, cool, and weigh as pyrophosphate of magnesia 2(MgO)P 2 5 .


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