The Chemistry And Technology of the Diazo Compounds

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The Chemistry And Technology of the Diazo Compounds
John Cannell Cain
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N 3, is obtained by treating aminoguanidine dinitrate with sodium nitrite in the presence of acetic acid (compare p. 128;. 5 1 Angeli, Ber. , 1893, 26, 1715; Gazzetta, 1895, 25, ii, 494.
2 Wolff, Annalen, 1912, 394, 23.
3 Prepared by treating sodium azoimide with methyl sulphate (Dimroth and Wislicenus, Ber. , 1905, 38, 1573).
4 Dimroth, Ber. , 1906, 39, 3905 ; compare ibid. , 1905, 38, 670. The first aliphatic diazoamino-compound was prepared by Thiele and Osborne, Annalen, 1899, 305, 64.
5 K.
... A. Hofmann and Hock, Ber. , 1910, 43, 1866.
DIAZO-COMPOUNDS OF ALIPHATIC SERIES 131 6. Azo-compounds of the aliphatic series. Azomethane, CH, . N : N. CH 3, is prepared by oxidising s-dimethylhydrazine dihydrochloride with potassium chromate. It is a colourless gas, very readily soluble in water, solidifies a little below -78 to colourless leaflets, and boils at l-8/756 mm. 1 Other azo-compounds of the aliphatic series, as well as some azoxy-compounds, have been described.
1 Thiele, Ber. , 1909, 42, 2575.


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