A Text-Book of Practical Chemistry

Cover A Text-Book of Practical Chemistry
A Text-Book of Practical Chemistry
Hood, George Frederic
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Evaporate on the toater-bathy moisten the residue with strong hydrochloric acid, dry again, again moisten with hydrochloric acid and set aside for half an hour. Dilute with 150 c.cs. water, boil, filter off the silicic acid, wash it and ignite it wet. Weigh as SiOj.
Note, — If the silica is pink, it contains ferric oxide. If it is grey it contains graphite.
In the first case fuse with fusion mixture. In the second case fuse with fusion mixture and potassium nitrate. Dissolve the melt in water,
...acidify strongly with hydrochloric acid, evaporate on the water-bath and treat as before. (Remember, two filter ashes.) Determination of phosphoms. — It is usual to determine the phosphorus in the same operation. The filtrate from the silica will contain it as phosphoric acid. It is evaporated dry, dissolved in the minimum of nitric acid and pptd.
by Woy's method, page 197.
Hydrofluoric aeid. Penfidd's method, — The fluoride is mixed with ten times its weight of finely powdered and ignited quartz and decomposed in a flask fitted with tap-funnel and delivery tube by heating with strong sul- phuric acid.


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