Ammonia And Ammonium Compounds : Comprising Their Manufacture From Gas-Liquor, And From Spent-Oxide ; a Practical Manual for Manufacturers, Chemists, Gas-Engineers, And Drysalters, From Personal Experience, And Including the Most Recent Discoveries And Im

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Let us suppose that 20 cc.
of the neutralized caustic soda extract (diluted pre- viously to 500 cc.) require 30 cc. of ferric chloride solu- tion, thenas 1000 cc. ferric chloride solution correspond to 2i'2 ferrocyanogen (Fe(CN)6) the whole extract 21-2 X in enn contains -1::^ f^_500 _ j.^ grms. =2x5-3 = 106 20 per cent, of ferrocyanogen.
Estimation of Ammonia. — This estimation is best II 98 Utilization of Spent-Oxide.
performed by the azotometric method (p. 25). For the total ammonia 3 — 4 gr
...ms. of the spent-oxide are weighed out and placed in the inner cylinder of the apparatus, and the analysis performed in the usual manner. To determine the quantity of soluble am- monia, 50 grms. of spent-oxide are extracted with water, the extract diluted to 200 or 250 cc, and 10 cc. analyzed by the azotometer.
(^.) Recovery of Sulphocyanides. — The recovery of sulphocyanides from spent-oxide forms at the present time a small but flourishing industry, the process being carried out by about ten different firms.


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