Analytical Chemistry volume 2

Cover Analytical Chemistry volume 2
Analytical Chemistry volume 2
F P Frederick Pearson Treadwell
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Care should be taken that the carbon on the asbestos reaches far enough into the tube to get the full heat from the furnace. The burners under the pre-heating furnace are now lighted, the oxygen turned on and allowed to pass through the absorption bulb at the rate of three bubbles per second, but no faster. The two forward burners under the combustion tube are lighted, at first turning them low and gradually raising the heat until the tube is hot. As soon as this end of the tube is hot, the thi...rd burner from the forward end is lighted and a few minutes later the fourth burner, which should be near the forward end of the carbon residue. Light each burner in succession until finally all are lighted and turned high enough to heat the tube red hot. After twenty minutes have elapsed from the time the last burner is turned on full, the oxygen is stopped and a current of air swept through the tube at the same rate for twenty minutes longer, gradually turning down the burners under the com- bustion tube.

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