Catalytic Hydrogenation And Reduction
Catalytic Hydrogenation And Reduction
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, 1905, 140, 482.
2 Paal and Gerum, Ber. , 1909, 42, 1553.
3 Skita, Ber. , 1909, 42, 1636.
MISCELLANEOUS REDUCTIONS 67 Reduction of Isonitriles.
Isonitriles, on being subjected to catalytic hydro- genation, give, in accordance with their constitu- tion, a reaction product differing essentially from that obtained from the corresponding nitrile. Sabatier and Mailhe, 1 who studied the reduction of aliphatic carbylamines by distillation with hydrogen over nickel, obtained, in general, a reaction of... the following type : CH 3 -N:C+2H 2 == CH 3 -NH-CH 3 .
It was found that a copper catalyst could be substituted for the nickel, but was less active. 2 The course of the reduction should be compared with that of the true nitriles described above.
Reduction of Isocyanic Esters.
Ethyl isocyanate, on being distilled with hydrogen over nickel at 250-290 C. , was converted princi- pally into secondary methyl-ethyl-amine. 3 O:C:N-C 2 H 5 +3H 2 = CH 3 *NH-C 2 H 5 +H 2 O Reduction of the -N:N- Group.
Skita 4 dissolved 9 grams of azobenzene in 250 c.
What to read after Catalytic Hydrogenation And Reduction?
You can find similar books in the "Read Also" column, or choose other free books by Edward B Edward Bradford Maxted to read onlineMoreLess
To quickly assess the difficulty of the text, read a short excerpt:
, 1905, 140, 482.
2 Paal and Gerum, Ber. , 1909, 42, 1553.
3 Skita, Ber. , 1909, 42, 1636.
MISCELLANEOUS REDUCTIONS 67 Reduction of Isonitriles.
Isonitriles, on being subjected to catalytic hydro- genation, give, in accordance with their constitu- tion, a reaction product differing essentially from that obtained from the corresponding nitrile. Sabatier and Mailhe, 1 who studied the reduction of aliphatic carbylamines by distillation with hydrogen over nickel, obtained, in general, a reaction of... the following type : CH 3 -N:C+2H 2 == CH 3 -NH-CH 3 .
It was found that a copper catalyst could be substituted for the nickel, but was less active. 2 The course of the reduction should be compared with that of the true nitriles described above.
Reduction of Isocyanic Esters.
Ethyl isocyanate, on being distilled with hydrogen over nickel at 250-290 C. , was converted princi- pally into secondary methyl-ethyl-amine. 3 O:C:N-C 2 H 5 +3H 2 = CH 3 *NH-C 2 H 5 +H 2 O Reduction of the -N:N- Group.
Skita 4 dissolved 9 grams of azobenzene in 250 c.
What to read after Catalytic Hydrogenation And Reduction?
You can find similar books in the "Read Also" column, or choose other free books by Edward B Edward Bradford Maxted to read onlineMoreLess
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