Experimental Organic Chemistry
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In our eReader you can find the full English version of the book. Read Experimental Organic Chemistry Online - link to read the book on full screen. Our eReader also allows you to upload and read Pdf, Txt, ePub and fb2 books. In the Mini eReder on the page below you can quickly view all pages of the book - Read Book Experimental Organic Chemistry
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(See Fig. 14, page 25. ) At the end of this time, arrange the apparatus for distillation, using a water condenser and having a thermometer to record the temperature of the vapor. Distil into a flask; when the temperature registers 100, collect separately about 1 cc. Of the distillate and add it to about 5 cc. Of water. If the mixture does not separate into two layers, stop the dis- tillation. Shake the distillate in the flask with 30 cc. Of water, and add solid sodium carbonate until a drop of ...the ester is neutral to moist litmus paper. Transfer to a separatory funnel, draw off the water, and shake the ester twice with a saturated solution of calcium chloride, using 50 cc. Each time. Draw off the ester into a distilling flask, add about one-fourth its volume of an- hydrous calcium chloride, close the flask and cover the side-arm with corks, and let stand for at least 1 hour. Distil from a water-bath. Note the boiling-point and the weight of ester ob- tained, and calculate the percentage yield from the acetic acid used.
What to read after Experimental Organic Chemistry?
You can find similar books in the "Read Also" column, or choose other free books by James Flack Norris to read onlineMoreLess
To quickly assess the difficulty of the text, read a short excerpt:
(See Fig. 14, page 25. ) At the end of this time, arrange the apparatus for distillation, using a water condenser and having a thermometer to record the temperature of the vapor. Distil into a flask; when the temperature registers 100, collect separately about 1 cc. Of the distillate and add it to about 5 cc. Of water. If the mixture does not separate into two layers, stop the dis- tillation. Shake the distillate in the flask with 30 cc. Of water, and add solid sodium carbonate until a drop of ...the ester is neutral to moist litmus paper. Transfer to a separatory funnel, draw off the water, and shake the ester twice with a saturated solution of calcium chloride, using 50 cc. Each time. Draw off the ester into a distilling flask, add about one-fourth its volume of an- hydrous calcium chloride, close the flask and cover the side-arm with corks, and let stand for at least 1 hour. Distil from a water-bath. Note the boiling-point and the weight of ester ob- tained, and calculate the percentage yield from the acetic acid used.
What to read after Experimental Organic Chemistry?
You can find similar books in the "Read Also" column, or choose other free books by James Flack Norris to read onlineMoreLess
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