Formation of Aluminium Nitride

Cover Formation of Aluminium Nitride
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At present the decomposition temperature of aluminum nitride is claimed to be somewhat lower.
- 9 EXPERIMENTAL WORK, With the idea in mind that the formation of aluminum nitride was commercially as well as experimentally possible, we set out to make the above a foregone conclusion. In order to do this it was necessary that the best quan- tities of raw materials, the best catalytic agent, the best temperature and time for forma- tion, and the flow and purity of nitrogen be ascertained. To gain t
...his knowledge it was decided to pass a stream of nitrogen over a finely divided mixtxire of bauxite, carbon, and the catalytic agent varying the temperature and percentage of constituents, the reaction to be carried on in an electric furnace. After this knowledge should be obtained the reaction was to be carried out on a larger scale and the process was to be made continuous.
The same electric furnace - a Hoskins carbon resistance fvirnace - was used in both preliminary and final operations. A graphite tube 30 inches long, 2^ inches wide and l/4 inch - 10 - thick, resting on two sets of transite rollers, formed the core and reaction chamber of the furnace.


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