Guide to the Analysis of Potable Spirits
Guide to the Analysis of Potable Spirits
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To this quan- THE ESTIMATION OF THE HIGHER ALCOHOLS 43 tity are added 3 grammes of chlorohydrate of meta- phenylenediamine or of phosphate of aniline (i c. C. Of phosphoric acid having a density of 1*453, and i c. C. Of pure aniline oil). Hewitt's reagent (see p. 22) answers this purpose well and most con- veniently. A few small pieces of pumice-stone are put in to control the ebullition, the flask is then attached to a reflux condenser, and its contents allowed to boil for one hour, so as to f...ix the alde- hydes. The contents of the flask are then distilled. The distillation is allowed to proceed rapidly over a naked flame, but not so far as to char the residue. The distillate is then brought up to its original volume, and the colorimetric tests applied to it. For developing the colour, 10 c. C. Of the distillate are placed in a scrupulously clean flask, and 10 c. C. Of monohydrated pure and colourless sulphuric acid are added by means of a pipette. The acid is allowed to trickle slowly from the pipette down the neck of the flask, so that it mixes with the alcohol without developing any marked degree of heat.
What to read after Guide to the Analysis of Potable Spirits?
You can find similar books in the "Read Also" column, or choose other free books by S Archibald Vasey to read onlineMoreLess
To quickly assess the difficulty of the text, read a short excerpt:
To this quan- THE ESTIMATION OF THE HIGHER ALCOHOLS 43 tity are added 3 grammes of chlorohydrate of meta- phenylenediamine or of phosphate of aniline (i c. C. Of phosphoric acid having a density of 1*453, and i c. C. Of pure aniline oil). Hewitt's reagent (see p. 22) answers this purpose well and most con- veniently. A few small pieces of pumice-stone are put in to control the ebullition, the flask is then attached to a reflux condenser, and its contents allowed to boil for one hour, so as to f...ix the alde- hydes. The contents of the flask are then distilled. The distillation is allowed to proceed rapidly over a naked flame, but not so far as to char the residue. The distillate is then brought up to its original volume, and the colorimetric tests applied to it. For developing the colour, 10 c. C. Of the distillate are placed in a scrupulously clean flask, and 10 c. C. Of monohydrated pure and colourless sulphuric acid are added by means of a pipette. The acid is allowed to trickle slowly from the pipette down the neck of the flask, so that it mixes with the alcohol without developing any marked degree of heat.
What to read after Guide to the Analysis of Potable Spirits?
You can find similar books in the "Read Also" column, or choose other free books by S Archibald Vasey to read onlineMoreLess
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