Laboratory Manual of Inorganic Chemistry : One Hundred Topics in General, Qualitative And Quantitative Chemistry

Cover Laboratory Manual of Inorganic Chemistry : One Hundred Topics in General, Qualitative And Quantitative Chemistry
Laboratory Manual of Inorganic Chemistry : One Hundred Topics in General, Qualitative And Quantitative Chemistry
Williams, Rufus P. (Rufus Phillips), 1851-1911
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67. IODIN.
Supplies: iodin, alcohol, sols, of KI and starch, KC10», HC1, test tubes.
1. Pour 4 or 5 CC of alcohol, C 2 H 6 OH, into the t.t. con- taining the sublimed iodin (Exp. 66), and shake the contents very vigorously. Warm the tube if necessary. State the effect on the alcohol and on the iodin. What does this exp. show you about the solubility of iodin ? The product is called tincture of iodin.
2. Prepare 5 or 10 cc of euchlorin (Exp. 64) in a t.t. for use in the following.
3. Pour into a
... clean t.t. 3 or 4 drops of potassium iodid sol., KI, and 2 or 3 drops of starch sol. (Exp. 65). Add 5 CC of H 2 0, and shake the contents. Now dip a s.r.
into the euchlorin, and in this way stir a drop of the euchlorin into the starch and It I sol. If there is no vis- ible effect, repeat the last operation with another drop of euchlorin. Describe in full, and explain with an equation to show the relative affinities of I and CI for K. Boil the sol., and note the effect, then cool it with a jet of water.


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