Quantitative Analysis for Mining Engineers

Cover Quantitative Analysis for Mining Engineers
Quantitative Analysis for Mining Engineers
Edmund H Edmund Howd Miller
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Weigh out half a gram of the sample, place this in a casserole, add about 20 c. C. Of water and stir well, then 15-20 c. C. Of strong hydrochloric acid, heat to boiling, while stirring to break up any lumps ; then evap- orate rapidly to dryness and bake, take up with hydrochloric acid and water, boil and filter, ignite and weigh the silica (impure). In the filtrate the alumina is precipitated, together with ferric hy- droxide, by ammonia and ammonium chloride. This should be reprecipitated, to ...free it from lime and magnesia, then ignited and weighed as usual.
* See also Lord's "Notes on Metallurgical Analysis, " p. 201 and seq.
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