Solvatochromic Investigations of Chromatographic Processes
Solvatochromic Investigations of Chromatographic Processes
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115 The slope of this isotherm was nearly equal to 1 (0.986), suggesting almost complete adsorption onto the surface. A similar isotherm was also done on 15% water added to the alumina (activity grade V) and a linear relationship with a slope of 0.685 was found. A smaller slope with activity grade V makes sense since more active sites have been occupied by water in the form of hydration reactions and bulk adsorption. Because the dye can dimerize, however, the lack of a plateau does not suggest ...a monolayer was not exceeded.
Spectral analysis as a function of the amount of dye adsorbed was also needed to truly determine if any self-association would occur. Figure 4-3 is a series of overlayed ET-30 on alumina spectra showing the effects of increased dye concentration on the charge-transfer band. The measured polarity did not change at all for the four lowest concentrations (95.3 to 379 mg ET-30 added/kg alumina) . At the two higher levels (474 and 572 mg/added) , the peaks became broader and began shifting to longer wavelengths.
What to read after Solvatochromic Investigations of Chromatographic Processes?
You can find similar books in the "Read Also" column, or choose other free books by Michels, James Joseph, 1962- to read onlineMoreLess
To quickly assess the difficulty of the text, read a short excerpt:
115 The slope of this isotherm was nearly equal to 1 (0.986), suggesting almost complete adsorption onto the surface. A similar isotherm was also done on 15% water added to the alumina (activity grade V) and a linear relationship with a slope of 0.685 was found. A smaller slope with activity grade V makes sense since more active sites have been occupied by water in the form of hydration reactions and bulk adsorption. Because the dye can dimerize, however, the lack of a plateau does not suggest ...a monolayer was not exceeded.
Spectral analysis as a function of the amount of dye adsorbed was also needed to truly determine if any self-association would occur. Figure 4-3 is a series of overlayed ET-30 on alumina spectra showing the effects of increased dye concentration on the charge-transfer band. The measured polarity did not change at all for the four lowest concentrations (95.3 to 379 mg ET-30 added/kg alumina) . At the two higher levels (474 and 572 mg/added) , the peaks became broader and began shifting to longer wavelengths.
What to read after Solvatochromic Investigations of Chromatographic Processes?
You can find similar books in the "Read Also" column, or choose other free books by Michels, James Joseph, 1962- to read onlineMoreLess
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