The Analysis of Fuel Gas Water And Lubricants

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capacity. Add water and cover the beaker with a watch glass. After solution is complete rinse and remove the fusion cup and add concentrated HCl to the neutral point. This will require 25 to 30 cc. of acid. Add about 1 cc. of normal acid in excess, filter if necessary, wash and make up the solution to about 225 cc. Precipitate the sulphates by means of barium chloride exactly as indicated under (a). Particular attention should be observed in washing the precipitate obtained by this method in or...der to remove all of the soluble salts which are formed in the fusion process.
(d) The photometric method for arriving at the factor for sulphur is extensively used and has many features of advantage especially in technical work. It is applicable to any of the solu- tions obtained under (a), (b), or (c) above, at that point where the solution is ready for precipitation by means of barium chloride. It is especially advantageous in method (c) where the peroxide fusion has been employed for the reason that separation from the heavy alkaline salts is not involved.


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