The Analysis of Paints And Painting Materials

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It depends on the heat developed by the mixing of the oil with strong sulphuric acid and is carried out as follows : 56 ANALYSIS OF PAINTS AND PAINTING MATERIALS.
A beaker of about 150 c. C. Capacity and from 7 1/2 to 9 cm. Deep is carefully placed into a larger vessel and surrounded with dry felt or cotton waste.
Fifty grams of the oil are put into the beaker and 10 c. C. Of concentrated sulphuric acid are gradually introduced into the oil from a burette and the mixture stirred until no furthe
...r in- crease in temperature is recorded by a thermometer immersed in it.
The highest point at which the thermometer remains con- stant for any appreciable time is observed, and the difference be- tween this and the initial temperature is the rise of temperature.
In performing this test, it is highly important that the oil and acid be originally of the same temperature and that the strength of the acid should be the same as far as possible.
As the rise in temperature varies with the strength of the acid, to secure uniformity the results should be expressed by dividing the rise of temperature with the oil by the rise of temperature with water and multiplying by 100.


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