The Molecular Rearrangement of Symmetrical Bis Triphenylmethylhydrazine
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To quickly assess the difficulty of the text, read a short excerpt:
ZnCli G.
Temp.
Time Min.
Found G.
Calc. G.
(CH*)j = C = N C 12 17 0. 50 0. 50 5 5 300 330 10 5 0. 005 0. 015 0. 09 0. 09 6 78. 5 17 90. 4 19 0. 61 6 330 3 0. 024 0. 11 22 . Vl'- : 21 0. 59 6 + 360 3 0. 032 0. 11 30 22 23 0. 51 0. 52 6+ 7 400 390+ 3 2 0. 030 0. 033 0. 09 0. 09 33 37 91. 3 04 0. 55 7 390+ 4 0. 031 0. 10 31 ^r 25 28 29 0. 51 0. 78 0. 57 7 7 7 390 + 450 450 2 2 0. 028 0. 038 0. 029 0. 09 0. 14 0. 10 31 27 29 approxi- mately 90 30 0. 57 7 450 ! X /6 0. 035 0. 10 35 32 0. 52 7 450 ! ...1 /6 0. 031 0. 09 34 These values are calculated on the basis of the assumption (Scheme I, p. 4 of the introduction) that each molecule of hydrazine yields one molecule of aniline i not two molecules (as demanded by Scheme II).
The method used in Expts. 30 and 32 was chosen as the best under the working conditions employed. Expt. 23 gave a better yield, but 60cc, flasks of the variety which after careful annealing would stand being plunged repeatedly into a metal bath at the temperatures used were then immediately available.
What to read after The Molecular Rearrangement of Symmetrical Bis Triphenylmethylhydrazine?
You can find similar books in the "Read Also" column, or choose other free books by Ralph Lyman Brown to read onlineMoreLess
To quickly assess the difficulty of the text, read a short excerpt:
ZnCli G.
Temp.
Time Min.
Found G.
Calc. G.
(CH*)j = C = N C 12 17 0. 50 0. 50 5 5 300 330 10 5 0. 005 0. 015 0. 09 0. 09 6 78. 5 17 90. 4 19 0. 61 6 330 3 0. 024 0. 11 22 . Vl'- : 21 0. 59 6 + 360 3 0. 032 0. 11 30 22 23 0. 51 0. 52 6+ 7 400 390+ 3 2 0. 030 0. 033 0. 09 0. 09 33 37 91. 3 04 0. 55 7 390+ 4 0. 031 0. 10 31 ^r 25 28 29 0. 51 0. 78 0. 57 7 7 7 390 + 450 450 2 2 0. 028 0. 038 0. 029 0. 09 0. 14 0. 10 31 27 29 approxi- mately 90 30 0. 57 7 450 ! X /6 0. 035 0. 10 35 32 0. 52 7 450 ! ...1 /6 0. 031 0. 09 34 These values are calculated on the basis of the assumption (Scheme I, p. 4 of the introduction) that each molecule of hydrazine yields one molecule of aniline i not two molecules (as demanded by Scheme II).
The method used in Expts. 30 and 32 was chosen as the best under the working conditions employed. Expt. 23 gave a better yield, but 60cc, flasks of the variety which after careful annealing would stand being plunged repeatedly into a metal bath at the temperatures used were then immediately available.
What to read after The Molecular Rearrangement of Symmetrical Bis Triphenylmethylhydrazine?
You can find similar books in the "Read Also" column, or choose other free books by Ralph Lyman Brown to read onlineMoreLess
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