The Practical Assayer, Containing Easy Methods for the Assay of the Principal Metals And Alloys, Principally Designed for Explorers And Those Interested in Mines
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of liquid are gradually distilled over into a beaker (by means of a bent tube fixed on to the end of the retort) which contains 100 C. C. of sulphuric acid, diluted to the required strength. As soon as 50 or 60 C. C. have passed over, allow the retort to eool, and 40 C. C. of water are added 190 THE PRACTICAL ASSAYER. to the retort ; distil again till this 40 C. C. has passed over, and once more repeat the same operation. A few drops of litmus are now added to the contents of the beaker, and th...e acid is neutralized by the standard alkali (caustic soda). This solution should be of such a strength that i C. C. equals an equal amount of acid solution originally introduced into the beaker. Suppose, now, this acid solution in the flask requires 67 C.C. of alkali solution, instead of 100. It is evident that 33 C. C. have been neutralized by the ammonia ; a quantity of ammonia has passed over therefore = to 3*3 grammes of anhydrous soda. From the two equivalents of the two alkalies, we may cal- culate the ammonia thus : Na20 H3N 31 : 17 : : 3"3 : I'Sog x ip or 1 8 -09 per cent, of ammonia in the sample, if 10 grammes are taken.
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