The Practical Methods of Organic Chemistry

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Before the heating is begun, a portion of the mixture is placed in a porcelain dish, the end of the stem of the funnel immersed in it and filled by suction. The cock is then closed, the funnel placed in the cork of the generating flask, and the heating begun.
ALIPHATIC SERIES 1 93 (fr) From Ethyl Alcohol and Phosphoric Acid Separation of carbon and foaming will be prevented in the preparation of ethylene when syrupy phosphoric acid is used in place of sulphuric acid. A 200 c. C. Round flask, wi
...th a wide mouth, is provided with a three-hole cork. Through one hole passes a thermometer extending to the bottom of the flask, through the second hole is inserted a dropping funnel ; the stem of the latter is at least 25 cm. Long and is drawn to a fine point. The end of the stem is kept only a few millimetres below the stopper. Through the third hole passes a delivery tube, not too narrow, bent at right angles. The tube is attached with rubber to a Wolfe flask, pro- vided with two tubulures flush with the stoppers.

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