The Technical Analysis of Brass And the Non Ferrous Alloys
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W. Clark's method of precipitation by hydrogen sulphide gas in a hot solution saturated with oxalic acid. The volume of the solution should not be over 25 to 50 cc.
Antimony sulphide is ignited in a porcelain cru- cible to the tetroxide.
Selenium and Tellurium. These elements are usually determined in a separate sample by the method of Edward Keller. The impurities are separated by precipitation with ferric hydroxide, which must be in large excess, and the selenium and tellurium are finally pre...cipitated from a hydro- chloric acid solution with sulphurous acid gas. Where a separation of the two is not desired, it is quicker and more convenient to precipitate them by stannous chloride. It is most accurate to filter and dry the selenium or tellurium on thin felts of the best asbestos and, after weighing them, to ignite and determine the elements by loss as a check. Dr. H. F. Keller has recommended hydroxylamine as a precipitant.
Lead, Iron, Zinc, Nickel and Cobalt. The bulk of the copper is removed by electrolysis and any deposit of lead peroxide on the anode is weighed.
What to read after The Technical Analysis of Brass And the Non Ferrous Alloys?
You can find similar books in the "Read Also" column, or choose other free books by William B William Benham Price to read onlineMoreLess
To quickly assess the difficulty of the text, read a short excerpt:
W. Clark's method of precipitation by hydrogen sulphide gas in a hot solution saturated with oxalic acid. The volume of the solution should not be over 25 to 50 cc.
Antimony sulphide is ignited in a porcelain cru- cible to the tetroxide.
Selenium and Tellurium. These elements are usually determined in a separate sample by the method of Edward Keller. The impurities are separated by precipitation with ferric hydroxide, which must be in large excess, and the selenium and tellurium are finally pre...cipitated from a hydro- chloric acid solution with sulphurous acid gas. Where a separation of the two is not desired, it is quicker and more convenient to precipitate them by stannous chloride. It is most accurate to filter and dry the selenium or tellurium on thin felts of the best asbestos and, after weighing them, to ignite and determine the elements by loss as a check. Dr. H. F. Keller has recommended hydroxylamine as a precipitant.
Lead, Iron, Zinc, Nickel and Cobalt. The bulk of the copper is removed by electrolysis and any deposit of lead peroxide on the anode is weighed.
What to read after The Technical Analysis of Brass And the Non Ferrous Alloys?
You can find similar books in the "Read Also" column, or choose other free books by William B William Benham Price to read onlineMoreLess
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