Victor Von Richter's Organic Chemistry ; Or, Chemistry of the Carbon Compounds
Victor Von Richter's Organic Chemistry ; Or, Chemistry of the Carbon Compounds
Victor Von Richter
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The most suitable oxidants are chromic acid, dilute nitric acid, potassium permanganate, and potassium ferricyanide. (a) Oxidation with Chromic Add, — Only the para- and meta-derivatives (the former more readily than the latter^ of benzenes, carrying two side-chains, are oxidized to acids by chromic acid, while the ortho- are either not attacked at all or are completely destroyed. In snbstitnted alkyl benzenes the alkyl -group is prevented from being oxidized by chromic acid, if a negative grou...p occup3ring the o-position with reference to the alkyl - group is present (B. 15, 1021). The oxidations are conducted either with free chromic acid in glacial acetic acid, or with a mixture of potassium bichromate (3 parts) and sul- phuric add (3 parts), diluted with 2-3 volumes of water. (h) Oxidation with Nitric Acid, — When oxidizing with nitric acid use acid diluted with 3 parts of water and boil for some time, hi connection with a return condenser (2-3 days). Kooowaloff (p. 178) contends that phenylnitroparaffins are 6rst produced ; these then are farther oxidized to carboxylic acids.
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